Kraft pulp cellulose was hydrolyzed using sulfuric acid under different thermophysical conditions of temperature time pulp concentration and sonication time The experimental design revealed the effect of these conditions and their interaction on the hydrolysis yield obtained In addition the top five cellulose nanocrystals CNCs yields from this experiment design were analyzed The
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Get PriceAngular scanning was conducted from 5° to 50° with 5° min −1 with Cu Kα radiation λ = nm and the generator worked at 45 kV and 200 mA The Segal Crystanillity index was calculated according to Equation 1 where I t is the total intensity of the 0 0 2 peak for cellulose I and I a is the amorphous intensity [ 31 ]
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